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Crystal Structures of Seven Terephthaldiamide Derivatives
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| Zeitschriftentitel: | Zeitschrift für Naturforschung B |
|---|---|
| Personen und Körperschaften: | , , |
| In: | Zeitschrift für Naturforschung B, 57, 2002, 8, S. 914-921 |
| Format: | E-Article |
| Sprache: | Englisch |
| veröffentlicht: |
Walter de Gruyter GmbH
|
| Schlagwörter: |
| author_facet |
Jones, P. G. Ossowski, J. Kus, P. Jones, P. G. Ossowski, J. Kus, P. |
|---|---|
| author |
Jones, P. G. Ossowski, J. Kus, P. |
| spellingShingle |
Jones, P. G. Ossowski, J. Kus, P. Zeitschrift für Naturforschung B Crystal Structures of Seven Terephthaldiamide Derivatives General Chemistry |
| author_sort |
jones, p. g. |
| spelling |
Jones, P. G. Ossowski, J. Kus, P. 1865-7117 0932-0776 Walter de Gruyter GmbH General Chemistry http://dx.doi.org/10.1515/znb-2002-0812 <jats:p>N,N′-Dibutyl-terephthaldiamide (1), N,N′-dihexyl-terephthaldiamide (2), N,N′-di(tert-butyl)- terephthaldiamide (3), N,N,N′,N′-tetrabutyl-terephthaldiamide (4), 1,1′-terephthaloylbis- pyrrolidine (5), 1,1′-terephthaloyl-bis-piperidine (6), and 4,4′-terephthaloyl-bis-morpholine (7) have been synthesised and physicochemically characterised. The X-ray structure determinations reveal imposed inversion symmetry for compounds 1-6; compound 3 has two independent molecules with inversion symmetry in the asymmetric unit. Compounds 1-3 form classical hydrogen bonds of the type N-H···O=C, leading to a ribbon-like arrangement of molecules (1 and 2) or a layer structure (3). Compound 3 also displays a very short C-H···O interaction, a type of hydrogen bond that is also observed in compounds 4-7, which lack classical donors; thereby compounds 4-6 form layer structures and 7 a complex threedimensional network.</jats:p> Crystal Structures of Seven Terephthaldiamide Derivatives Zeitschrift für Naturforschung B |
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Crystal Structures of Seven Terephthaldiamide Derivatives |
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Crystal Structures of Seven Terephthaldiamide Derivatives |
| title_full |
Crystal Structures of Seven Terephthaldiamide Derivatives |
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Crystal Structures of Seven Terephthaldiamide Derivatives |
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Crystal Structures of Seven Terephthaldiamide Derivatives |
| title_short |
Crystal Structures of Seven Terephthaldiamide Derivatives |
| title_sort |
crystal structures of seven terephthaldiamide derivatives |
| topic |
General Chemistry |
| url |
http://dx.doi.org/10.1515/znb-2002-0812 |
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2002 |
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914-921 |
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<jats:p>N,N′-Dibutyl-terephthaldiamide (1), N,N′-dihexyl-terephthaldiamide (2), N,N′-di(tert-butyl)- terephthaldiamide (3), N,N,N′,N′-tetrabutyl-terephthaldiamide (4), 1,1′-terephthaloylbis- pyrrolidine (5), 1,1′-terephthaloyl-bis-piperidine (6), and 4,4′-terephthaloyl-bis-morpholine (7) have been synthesised and physicochemically characterised. The X-ray structure determinations reveal imposed inversion symmetry for compounds 1-6; compound 3 has two independent molecules with inversion symmetry in the asymmetric unit. Compounds 1-3 form classical hydrogen bonds of the type N-H···O=C, leading to a ribbon-like arrangement of molecules (1 and 2) or a layer structure (3). Compound 3 also displays a very short C-H···O interaction, a type of hydrogen bond that is also observed in compounds 4-7, which lack classical donors; thereby compounds 4-6 form layer structures and 7 a complex threedimensional network.</jats:p> |
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| description | <jats:p>N,N′-Dibutyl-terephthaldiamide (1), N,N′-dihexyl-terephthaldiamide (2), N,N′-di(tert-butyl)- terephthaldiamide (3), N,N,N′,N′-tetrabutyl-terephthaldiamide (4), 1,1′-terephthaloylbis- pyrrolidine (5), 1,1′-terephthaloyl-bis-piperidine (6), and 4,4′-terephthaloyl-bis-morpholine (7) have been synthesised and physicochemically characterised. The X-ray structure determinations reveal imposed inversion symmetry for compounds 1-6; compound 3 has two independent molecules with inversion symmetry in the asymmetric unit. Compounds 1-3 form classical hydrogen bonds of the type N-H···O=C, leading to a ribbon-like arrangement of molecules (1 and 2) or a layer structure (3). Compound 3 also displays a very short C-H···O interaction, a type of hydrogen bond that is also observed in compounds 4-7, which lack classical donors; thereby compounds 4-6 form layer structures and 7 a complex threedimensional network.</jats:p> |
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| spelling | Jones, P. G. Ossowski, J. Kus, P. 1865-7117 0932-0776 Walter de Gruyter GmbH General Chemistry http://dx.doi.org/10.1515/znb-2002-0812 <jats:p>N,N′-Dibutyl-terephthaldiamide (1), N,N′-dihexyl-terephthaldiamide (2), N,N′-di(tert-butyl)- terephthaldiamide (3), N,N,N′,N′-tetrabutyl-terephthaldiamide (4), 1,1′-terephthaloylbis- pyrrolidine (5), 1,1′-terephthaloyl-bis-piperidine (6), and 4,4′-terephthaloyl-bis-morpholine (7) have been synthesised and physicochemically characterised. The X-ray structure determinations reveal imposed inversion symmetry for compounds 1-6; compound 3 has two independent molecules with inversion symmetry in the asymmetric unit. Compounds 1-3 form classical hydrogen bonds of the type N-H···O=C, leading to a ribbon-like arrangement of molecules (1 and 2) or a layer structure (3). Compound 3 also displays a very short C-H···O interaction, a type of hydrogen bond that is also observed in compounds 4-7, which lack classical donors; thereby compounds 4-6 form layer structures and 7 a complex threedimensional network.</jats:p> Crystal Structures of Seven Terephthaldiamide Derivatives Zeitschrift für Naturforschung B |
| spellingShingle | Jones, P. G., Ossowski, J., Kus, P., Zeitschrift für Naturforschung B, Crystal Structures of Seven Terephthaldiamide Derivatives, General Chemistry |
| title | Crystal Structures of Seven Terephthaldiamide Derivatives |
| title_full | Crystal Structures of Seven Terephthaldiamide Derivatives |
| title_fullStr | Crystal Structures of Seven Terephthaldiamide Derivatives |
| title_full_unstemmed | Crystal Structures of Seven Terephthaldiamide Derivatives |
| title_short | Crystal Structures of Seven Terephthaldiamide Derivatives |
| title_sort | crystal structures of seven terephthaldiamide derivatives |
| title_unstemmed | Crystal Structures of Seven Terephthaldiamide Derivatives |
| topic | General Chemistry |
| url | http://dx.doi.org/10.1515/znb-2002-0812 |