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Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data
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| Zeitschriftentitel: | Acta Crystallographica Section E Crystallographic Communications |
|---|---|
| Personen und Körperschaften: | , |
| In: | Acta Crystallographica Section E Crystallographic Communications, 76, 2020, 4, S. 523-526 |
| Format: | E-Article |
| Sprache: | Unbestimmt |
| veröffentlicht: |
International Union of Crystallography (IUCr)
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| Schlagwörter: |
| author_facet |
Moon, Dohyun Choi, Jong-Ha Moon, Dohyun Choi, Jong-Ha |
|---|---|
| author |
Moon, Dohyun Choi, Jong-Ha |
| spellingShingle |
Moon, Dohyun Choi, Jong-Ha Acta Crystallographica Section E Crystallographic Communications Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data Condensed Matter Physics General Materials Science General Chemistry |
| author_sort |
moon, dohyun |
| spelling |
Moon, Dohyun Choi, Jong-Ha 2056-9890 International Union of Crystallography (IUCr) Condensed Matter Physics General Materials Science General Chemistry http://dx.doi.org/10.1107/s2056989020003059 <jats:p>The crystal structure of title compound, (C<jats:sub>14</jats:sub>H<jats:sub>36</jats:sub>N<jats:sub>4</jats:sub>)[CrO<jats:sub>3</jats:sub>Cl]<jats:sub>2</jats:sub>Cl<jats:sub>2</jats:sub>, has been determined by synchrotron radiation X-ray crystallography at 220 K. The macrocyclic cation lies across a crystallographic inversion center and hence the asymmetric unit contains one half of the organic cation, one chlorochromate anion and one chloride anion. Both the Cl<jats:sup>−</jats:sup> anion and chlorochromate Cl atom are involved in hydrogen bonding. In the crystal, hydrogen bonds involving the 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane (TMC) N—H groups and C—H groups as donor groups and three O atoms of the chlorochromate and the chloride anion as acceptor groups link the components, giving rise to a three-dimensional network.</jats:p> Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data Acta Crystallographica Section E Crystallographic Communications |
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10.1107/s2056989020003059 |
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Online Free |
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Physik |
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International Union of Crystallography (IUCr), 2020 |
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Acta Crystallographica Section E Crystallographic Communications |
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| title |
Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_unstemmed |
Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_full |
Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_fullStr |
Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_full_unstemmed |
Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_short |
Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_sort |
crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(vi)] dichloride from synchrotron x-ray data |
| topic |
Condensed Matter Physics General Materials Science General Chemistry |
| url |
http://dx.doi.org/10.1107/s2056989020003059 |
| publishDate |
2020 |
| physical |
523-526 |
| description |
<jats:p>The crystal structure of title compound, (C<jats:sub>14</jats:sub>H<jats:sub>36</jats:sub>N<jats:sub>4</jats:sub>)[CrO<jats:sub>3</jats:sub>Cl]<jats:sub>2</jats:sub>Cl<jats:sub>2</jats:sub>, has been determined by synchrotron radiation X-ray crystallography at 220 K. The macrocyclic cation lies across a crystallographic inversion center and hence the asymmetric unit contains one half of the organic cation, one chlorochromate anion and one chloride anion. Both the Cl<jats:sup>−</jats:sup> anion and chlorochromate Cl atom are involved in hydrogen bonding. In the crystal, hydrogen bonds involving the 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane (TMC) N—H groups and C—H groups as donor groups and three O atoms of the chlorochromate and the chloride anion as acceptor groups link the components, giving rise to a three-dimensional network.</jats:p> |
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| author | Moon, Dohyun, Choi, Jong-Ha |
| author_facet | Moon, Dohyun, Choi, Jong-Ha, Moon, Dohyun, Choi, Jong-Ha |
| author_sort | moon, dohyun |
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| container_title | Acta Crystallographica Section E Crystallographic Communications |
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| description | <jats:p>The crystal structure of title compound, (C<jats:sub>14</jats:sub>H<jats:sub>36</jats:sub>N<jats:sub>4</jats:sub>)[CrO<jats:sub>3</jats:sub>Cl]<jats:sub>2</jats:sub>Cl<jats:sub>2</jats:sub>, has been determined by synchrotron radiation X-ray crystallography at 220 K. The macrocyclic cation lies across a crystallographic inversion center and hence the asymmetric unit contains one half of the organic cation, one chlorochromate anion and one chloride anion. Both the Cl<jats:sup>−</jats:sup> anion and chlorochromate Cl atom are involved in hydrogen bonding. In the crystal, hydrogen bonds involving the 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane (TMC) N—H groups and C—H groups as donor groups and three O atoms of the chlorochromate and the chloride anion as acceptor groups link the components, giving rise to a three-dimensional network.</jats:p> |
| doi_str_mv | 10.1107/s2056989020003059 |
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| imprint | International Union of Crystallography (IUCr), 2020 |
| imprint_str_mv | International Union of Crystallography (IUCr), 2020 |
| institution | DE-Pl11, DE-Rs1, DE-105, DE-14, DE-Ch1, DE-L229, DE-D275, DE-Bn3, DE-Brt1, DE-Zwi2, DE-D161, DE-Gla1, DE-Zi4, DE-15 |
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| mega_collection | International Union of Crystallography (IUCr) (CrossRef) |
| physical | 523-526 |
| publishDate | 2020 |
| publishDateSort | 2020 |
| publisher | International Union of Crystallography (IUCr) |
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| series | Acta Crystallographica Section E Crystallographic Communications |
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| spelling | Moon, Dohyun Choi, Jong-Ha 2056-9890 International Union of Crystallography (IUCr) Condensed Matter Physics General Materials Science General Chemistry http://dx.doi.org/10.1107/s2056989020003059 <jats:p>The crystal structure of title compound, (C<jats:sub>14</jats:sub>H<jats:sub>36</jats:sub>N<jats:sub>4</jats:sub>)[CrO<jats:sub>3</jats:sub>Cl]<jats:sub>2</jats:sub>Cl<jats:sub>2</jats:sub>, has been determined by synchrotron radiation X-ray crystallography at 220 K. The macrocyclic cation lies across a crystallographic inversion center and hence the asymmetric unit contains one half of the organic cation, one chlorochromate anion and one chloride anion. Both the Cl<jats:sup>−</jats:sup> anion and chlorochromate Cl atom are involved in hydrogen bonding. In the crystal, hydrogen bonds involving the 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane (TMC) N—H groups and C—H groups as donor groups and three O atoms of the chlorochromate and the chloride anion as acceptor groups link the components, giving rise to a three-dimensional network.</jats:p> Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data Acta Crystallographica Section E Crystallographic Communications |
| spellingShingle | Moon, Dohyun, Choi, Jong-Ha, Acta Crystallographica Section E Crystallographic Communications, Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data, Condensed Matter Physics, General Materials Science, General Chemistry |
| title | Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_full | Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_fullStr | Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_full_unstemmed | Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_short | Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| title_sort | crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(vi)] dichloride from synchrotron x-ray data |
| title_unstemmed | Crystal structure of 1,4,8,11-tetramethyl-1,4,8,11-tetraazoniacyclotetradecane bis[chloridochromate(VI)] dichloride from synchrotron X-ray data |
| topic | Condensed Matter Physics, General Materials Science, General Chemistry |
| url | http://dx.doi.org/10.1107/s2056989020003059 |