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Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles
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| Veröffentlicht in: | Scientific reports Bd. 7.2017, 1, Art.-Nr. 73314, insges. 9 Seiten |
|---|---|
| Personen und Körperschaften: | , , , , , , , , , , , , , , |
| Titel: | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles/ Prokopios Georgopanos, Gerold A. Schneider, Axel Dreyer, Ulrich A. Handge, Volkan Filiz, Artur Feld, Ezgi D. Yilmaz, Tobias Krekeler, Martin Ritter, Horst Weller & Volker Abetz |
| Format: | E-Book-Kapitel |
| Sprache: | Englisch |
| veröffentlicht: |
2017
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| Gesamtaufnahme: |
: Scientific reports, Bd. 7.2017, 1, Art.-Nr. 73314, insges. 9 Seiten
, volume:7 |
| Quelle: | Verbunddaten SWB Lizenzfreie Online-Ressourcen |
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| 245 | 1 | 0 | |a Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles |c Prokopios Georgopanos, Gerold A. Schneider, Axel Dreyer, Ulrich A. Handge, Volkan Filiz, Artur Feld, Ezgi D. Yilmaz, Tobias Krekeler, Martin Ritter, Horst Weller & Volker Abetz |
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| 520 | |a In this work the fabrication of hard, stiff and strong nanocomposites based on polybutadiene and iron oxide nanoparticles is presented. The nanocomposites are fabricated via a general concept for mechanically superior nanocomposites not based on the brick and mortar structure, thus on globular nanoparticles with nanosized organic shells. For the fabrication of the composites oleic acid functionalized iron oxide nanoparticles are decorated via ligand exchange with an α,ω-polybutadiene dicarboxylic acid. The functionalized particles were processed at 145 °C. Since polybutadiene contains double bonds the nanocomposites obtained a crosslinked structure which was enhanced by the presence of oxygen or sulfur. It was found that the crosslinking and filler percolation yields high elastic moduli of approximately 12-20 GPa and hardness of 15-18 GPa, although the polymer volume fraction is up to 40%. We attribute our results to a catalytically enhanced crosslinking reaction of the polymer chains induced by oxygen or sulfur and to the microstructure of the nanocomposite. | ||
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| author | Georgopanos, Prokopios, Schneider, Gerold A., Dreyer, Axel, Handge, Ulrich A., Filiz, Volkan, Feld, Artur, Yılmaz, Ezgi D., Krekeler, Tobias, Ritter, Martin, Weller, Horst, Abetz, Volker |
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| contents | In this work the fabrication of hard, stiff and strong nanocomposites based on polybutadiene and iron oxide nanoparticles is presented. The nanocomposites are fabricated via a general concept for mechanically superior nanocomposites not based on the brick and mortar structure, thus on globular nanoparticles with nanosized organic shells. For the fabrication of the composites oleic acid functionalized iron oxide nanoparticles are decorated via ligand exchange with an α,ω-polybutadiene dicarboxylic acid. The functionalized particles were processed at 145 °C. Since polybutadiene contains double bonds the nanocomposites obtained a crosslinked structure which was enhanced by the presence of oxygen or sulfur. It was found that the crosslinking and filler percolation yields high elastic moduli of approximately 12-20 GPa and hardness of 15-18 GPa, although the polymer volume fraction is up to 40%. We attribute our results to a catalytically enhanced crosslinking reaction of the polymer chains induced by oxygen or sulfur and to the microstructure of the nanocomposite. |
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| spelling | Georgopanos, Prokopios VerfasserIn aut, Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles Prokopios Georgopanos, Gerold A. Schneider, Axel Dreyer, Ulrich A. Handge, Volkan Filiz, Artur Feld, Ezgi D. Yilmaz, Tobias Krekeler, Martin Ritter, Horst Weller & Volker Abetz, 2017, Illustrationen, Diagramme, Text txt rdacontent, Computermedien c rdamedia, Online-Ressource cr rdacarrier, In this work the fabrication of hard, stiff and strong nanocomposites based on polybutadiene and iron oxide nanoparticles is presented. The nanocomposites are fabricated via a general concept for mechanically superior nanocomposites not based on the brick and mortar structure, thus on globular nanoparticles with nanosized organic shells. For the fabrication of the composites oleic acid functionalized iron oxide nanoparticles are decorated via ligand exchange with an α,ω-polybutadiene dicarboxylic acid. The functionalized particles were processed at 145 °C. Since polybutadiene contains double bonds the nanocomposites obtained a crosslinked structure which was enhanced by the presence of oxygen or sulfur. It was found that the crosslinking and filler percolation yields high elastic moduli of approximately 12-20 GPa and hardness of 15-18 GPa, although the polymer volume fraction is up to 40%. We attribute our results to a catalytically enhanced crosslinking reaction of the polymer chains induced by oxygen or sulfur and to the microstructure of the nanocomposite., Schneider, Gerold A. VerfasserIn (DE-588)113530839X (DE-627)890264732 (DE-576)48976018X aut, Dreyer, Axel VerfasserIn (DE-588)1184595852 (DE-627)1663648689 aut, Handge, Ulrich A. VerfasserIn aut, Filiz, Volkan VerfasserIn aut, Feld, Artur VerfasserIn (DE-588)1145220142 (DE-627)100552517X (DE-576)495681431 aut, Yılmaz, Ezgi D. 1985- VerfasserIn (DE-588)1163572926 (DE-627)1027894135 (DE-576)50806273X aut, Krekeler, Tobias VerfasserIn (DE-588)107429033X (DE-627)831975741 (DE-576)442567006 aut, Ritter, Martin 1970- VerfasserIn (DE-588)132680440 (DE-627)525179410 (DE-576)263054462 aut, Weller, Horst 1954- VerfasserIn (DE-588)1024635481 (DE-627)720241855 (DE-576)369295641 aut, Abetz, Volker VerfasserIn (DE-588)140937501 (DE-627)622939270 (DE-576)321445740 aut, SFB 986 Maßgeschneiderte Multiskalige Materialsysteme M3 Sonstige Körperschaft (DE-588)115661807X (DE-627)1019408316 (DE-576)502290641 oth, Technische Universität Hamburg Sonstige Körperschaft (DE-588)1112763473 (DE-627)866918418 (DE-576)476770564 oth, Technische Universität Hamburg Institut für Keramische Hochleistungswerkstoffe Sonstige Körperschaft (DE-588)1156636019 (DE-627)1019441577 (DE-576)502338458 oth, Technische Universität Hamburg Betriebseinheit Elektronenmikroskopie BEEM Sonstige Körperschaft (DE-588)1156636221 (DE-627)1019442085 (DE-576)502338679 oth, Enthalten in Scientific reports [London] : Macmillan Publishers Limited, part of Springer Nature, 2011 Bd. 7.2017, 1, Art.-Nr. 73314, insges. 9 Seiten Online-Ressource (DE-627)663366712 (DE-600)2615211-3 (DE-576)346641179 2045-2322 nnns, volume:7 year:2017 number:1, https://doi.org/10.1038%2Fs41598-017-07521-0 Resolving-System Volltext, http://nbn-resolving.de/urn:nbn:de:gbv:830-88220377 Resolving-System kostenfrei Volltext, https://doi.org/10.15480/882.1626 Resolving-System kostenfrei Volltext, http://hdl.handle.net/11420/1629 Resolving-System kostenfrei Volltext, http://nbn-resolving.de/urn:nbn:de:gbv:830-88220377 LFER, LFER 2019-05-29T00:00:00Z |
| spellingShingle | Georgopanos, Prokopios, Schneider, Gerold A., Dreyer, Axel, Handge, Ulrich A., Filiz, Volkan, Feld, Artur, Yılmaz, Ezgi D., Krekeler, Tobias, Ritter, Martin, Weller, Horst, Abetz, Volker, Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles, In this work the fabrication of hard, stiff and strong nanocomposites based on polybutadiene and iron oxide nanoparticles is presented. The nanocomposites are fabricated via a general concept for mechanically superior nanocomposites not based on the brick and mortar structure, thus on globular nanoparticles with nanosized organic shells. For the fabrication of the composites oleic acid functionalized iron oxide nanoparticles are decorated via ligand exchange with an α,ω-polybutadiene dicarboxylic acid. The functionalized particles were processed at 145 °C. Since polybutadiene contains double bonds the nanocomposites obtained a crosslinked structure which was enhanced by the presence of oxygen or sulfur. It was found that the crosslinking and filler percolation yields high elastic moduli of approximately 12-20 GPa and hardness of 15-18 GPa, although the polymer volume fraction is up to 40%. We attribute our results to a catalytically enhanced crosslinking reaction of the polymer chains induced by oxygen or sulfur and to the microstructure of the nanocomposite. |
| title | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles |
| title_auth | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles |
| title_full | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles Prokopios Georgopanos, Gerold A. Schneider, Axel Dreyer, Ulrich A. Handge, Volkan Filiz, Artur Feld, Ezgi D. Yilmaz, Tobias Krekeler, Martin Ritter, Horst Weller & Volker Abetz |
| title_fullStr | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles Prokopios Georgopanos, Gerold A. Schneider, Axel Dreyer, Ulrich A. Handge, Volkan Filiz, Artur Feld, Ezgi D. Yilmaz, Tobias Krekeler, Martin Ritter, Horst Weller & Volker Abetz |
| title_full_unstemmed | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles Prokopios Georgopanos, Gerold A. Schneider, Axel Dreyer, Ulrich A. Handge, Volkan Filiz, Artur Feld, Ezgi D. Yilmaz, Tobias Krekeler, Martin Ritter, Horst Weller & Volker Abetz |
| title_in_hierarchy | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles / Prokopios Georgopanos, Gerold A. Schneider, Axel Dreyer, Ulrich A. Handge, Volkan Filiz, Artur Feld, Ezgi D. Yilmaz, Tobias Krekeler, Martin Ritter, Horst Weller & Volker Abetz, |
| title_short | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles |
| title_sort | exceptionally strong stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles |
| title_unstemmed | Exceptionally strong, stiff and hard hybrid material based on an elastomer and isotropically shaped ceramic nanoparticles |
| url | https://doi.org/10.1038%2Fs41598-017-07521-0, http://nbn-resolving.de/urn:nbn:de:gbv:830-88220377, https://doi.org/10.15480/882.1626, http://hdl.handle.net/11420/1629 |
| urn | urn:nbn:de:gbv:830-88220377 |